##TITLE=NP0000333, Submission ID 255, Experimental spectrum ##JCAMP-DX=4.24 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=LINK ##TITLE=Ureidosuccinic acid ##JCAMP-CS=3.7 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##BLOCK_ID=1 ##CROSS REFERENCE=NMR PEAK ASSIGNMENTS:BLOCK_ID=4 ##MOLFORM=C5 H8 N2 O5 ##ATOMLIST= 1 N 0 2 C 0 3 O 0 4 N 0 5 C 0 6 C 0 7 C 0 8 O 0 9 O 0 10 C 0 11 O 0 12 O 0 13 H 0 14 H 0 15 H 0 16 H 0 17 H 0 18 H 0 19 H 0 20 H 0 ##BONDLIST= 1 2 S 2 3 D 2 4 S 4 5 S 5 6 S 6 7 S 7 8 D 7 9 S 5 10 S 10 11 D 10 12 S 1 13 S 1 14 S 4 15 S 5 16 S 6 17 S 6 18 S 9 19 S 12 20 S ##STEREOCENTER= 5 P 0 ##$MOLFILE= RDKit 3D 20 19 0 0 0 0 0 0 0 0999 V2000 2.6936 1.6724 -0.3217 N 0 0 0 0 0 0 0 0 0 0 0 0 1.9742 0.5585 0.1827 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4492 -0.1306 1.0559 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6970 0.2702 -0.3653 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.1158 -0.8143 0.1732 C 0 0 1 0 0 0 0 0 0 0 0 0 -1.1277 -0.1826 1.1646 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9161 0.9028 0.6078 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.6870 1.5037 1.4410 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.9840 1.3707 -0.6800 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7377 -1.7169 -0.7547 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8715 -1.9297 -0.9644 O 0 0 0 0 0 0 0 0 0 0 0 0 0.1969 -2.4892 -1.5368 O 0 0 0 0 0 0 0 0 0 0 0 0 3.4029 1.6492 -1.0755 H 0 0 0 0 0 0 0 0 0 0 0 0 2.4948 2.5994 0.1934 H 0 0 0 0 0 0 0 0 0 0 0 0 0.3841 0.7655 -1.1966 H 0 0 0 0 0 0 0 0 0 0 0 0 0.5290 -1.4256 0.8654 H 0 0 0 0 0 0 0 0 0 0 0 0 -0.6367 0.0691 2.0715 H 0 0 0 0 0 0 0 0 0 0 0 0 -1.8475 -1.0499 1.3392 H 0 0 0 0 0 0 0 0 0 0 0 0 -2.8796 1.2387 -1.1326 H 0 0 0 0 0 0 0 0 0 0 0 0 0.9819 -2.8614 -1.0671 H 0 0 0 0 0 0 0 0 0 0 0 0 1 2 1 0 2 3 2 0 2 4 1 0 4 5 1 0 5 6 1 0 6 7 1 0 7 8 2 0 7 9 1 0 5 10 1 0 10 11 2 0 10 12 1 0 1 13 1 0 1 14 1 0 4 15 1 0 5 16 1 1 6 17 1 0 6 18 1 0 9 19 1 0 12 20 1 0 M END ##END= ##TITLE=Experimental spectrum ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR SPECTRUM ##BLOCK_ID=2 ##TEMPERATURE=NA ##.OBSERVE FREQUENCY=600 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##.SHIFT REFERENCE=INTERNAL,DSS,58937.00,0.0 ##XUNITS=PPM ##FIRSTX=10.803153756609914 ##LASTX=-1.2094135854575585 ##MINX=-1.2094135854575585 ##MAXX=10.803153756609914 ##XFACTOR=0.00018330002810884594 ##NPOINTS=65536 ##YUNITS=ARBITRARY UNITS ##FIRSTY=0.5219995558674096 ##LASTY=-5.004298476447707e-05 ##MINY=-830.992253485301 ##MAXY=10000.0 ##YFACTOR=0.3051850947599719 ##XYDATA=(X++(Y..Y)), XYDATA $$ DIF 58937B%%%%j%%%%%%%%%%%%%%%%%%%%%%j%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58863@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58789@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58715@%%%%%j%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58641@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%j%%%%%%%%%%%%%%%J%%% 58567A%%%%%%%%%%%%%%%%J%%%%%%j%%%%%%%%J%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58493A%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%% 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-2787A%%%%%%%%%%%J%%j%%%%%%%%%%%%%jJ%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%j%% -2861AJ%%%%%%%%%%%j%%%%%%%%J%%%%%%%%%j%%%%%%%%%%%%%%%%%%%J%%%%%%%%j%%J%%%%%j%%%% -2935A%%%%%%%%%%%%%J%%%%%j%%%%%%%%%%J%%%%%%%%j%%%%%%%%%%%%j%%J%%%%%%%%%%%%%%%%%% -3009A%%%%%%%%%%%%%%%j%%%%%%J%%%%%j%%%%%%%%%%%%%%%%%%%%%%J%%%%%j%%%%%%%%%%%%%J%% -3083A%%%%%%%%%%%j%%%%%%j%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%J%%%%j%%%%%%%% -3157a%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%j%%%%%%%%%%%%%%%%j%%% -3231a%%%%%%%%J%%%%j%%%%%%%%J%%%%%%%%j%%%%%%%%%%J%%%%%j%%%%%%%%%%%%%%%%%%%%%%J%j -3305a%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%j%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%J%% -3379A%%j%%%%%%%%%%%%%%%%j%%%%%%%J%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%% -3453aJ%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -3527@%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%j%%% -3601@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%j%%%%j%%J%%%%%%%%%J%%%%%%%%%%% -3675A%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%% -3749a%%%%J%%%%%%%j%%%%%%%%%%%J%%%%%%j%%%%%%%%%%%%%%%%%j%%%%%%%%%%%J%%%%%%%%%%%% -3823a%J%%j%%%%%%%%%%%%%%%%%%%J%j%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -3897@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -3971@%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%J%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -4045a%%%J%%%%%%%%%%%%%j%%%%J%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -4119aj%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%j%%%%%%%%%%%%%J%%%%%%%%%%%%%% -4193a%%%%%%%%%j%%%%%%%J%%%%%J%%%%%%%%%%%%%j%%%%%J%%%%j%%%%%%%%J%%%%%%%%%%%%%%%% -4267@%%j%%%%%%%J%%%%%%%%%j%%J%%%%%%%%%%%%%%%%%%j%%%%j%%%%J%%%%%%%%%j%%%%%%%J%%% -4341a%%%%%%%%J%%j%%%%j%%%%J%%%%%%%%j%%%%%%j%%%%%%J%%%%%%j%%%%%%J%%%%%%%%%%%%%%% -4415b%%%%%%%%%%%%%%%%%%J%%%%%j%%%%%%%%%%%J%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%% -4489@%j%%%%%%%%%%%J%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%J%%%%%% -4563A%%%j%%%%%J%%%%%%%%%%%%%%%%%%%%J%%%%%j%%%%%%%%%j%%%J%%j%%j%%%%%%%%%%%%%%J%% -4637@%%%%%%%%j%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -4711b%%%%%%J%%%%j%%%%%%J%%J%%j%%%%%%%%%J%%%%%%%%%%%%j%J%%%%%J%%%j%%%%%%%%%%%%%J -4785A%%j%%%%%%%J%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%j%%%%%%%%%%%%% -4859@%%%%%%%%%%%%%%J%%%%%j%%%%%j%%%J%%%%%%%%%%%%%%%jJ%%%%%%%%%%%%%%%j%%%%%%%%%% -4933a%%%%%%%%Jj%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5007@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%J%%%j%%%%%%%%% -5081a%%%%%%%%%%%j%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%% -5155b%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%J%%%%%%%%%%j%%%%%%%%%J%%%%%%%%j%%%% -5229b%%%%%%%%%%%%%%%%%J%%%%%%%j%%%%J%%%%%j%%%%%%Jj%%%%%%%%%%%%%J%%%J%%%%%jJ%%%% -5303@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5377@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%J%%%%%j%%%%J%%%%%%j%%%%%%%%%%%%%%%%% -5451A%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%J%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5525@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5599@%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%j%%%%%J%%%%%%%%%%%%%% -5673a%%%%%J%%%%%%%%%%%%%%%%%J%%%%%%%%j%%%%%%%%%%%%%%%%%%%%J%%%j%%%%%%%%%%%%%%%% -5747@%%%%%%%%%%%%%J%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%J%%%%%%%%%%%%%%%%%%%%%% -5821@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5895@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%J -5969@%%%%%j%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6043@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%J%%%%%%%%%%%%%% -6117@%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6191A%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6265@%%%%%%%%%%%%%%J%%%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%% -6339@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6413@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6487@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6561@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6598@ $$ checkpoint ##END= ##TITLE=Simulated peaks ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR PEAK TABLE ##DATA CLASS=PEAK TABLE ##BLOCK_ID=3 ##TEMPERATURE=NA ##.OBSERVE FREQUENCY=600 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##NPOINTS=12 ##XUNITS=PPM ##YUNITS=ARBITRARY UNITS ##PEAK TABLE=(XY..XY) (4.2335205078125, 144.13035990246647) (4.2257232666015625, 144.85347701644844) (4.2141876220703125, 145.14651189489348) (4.2064971923828125, 144.34524705475368) (2.475082397460937, 142.00913805870258) (2.455856323242187, 142.65802460882202) (2.4442138671874996, 143.05740586188728) (2.4249877929687496, 141.8331438753004) (2.679306030273437, 144.0049516400396) (2.671615600585937, 144.12603948222895) (2.6484374999999996, 144.1830356293766) (2.6407470703124996, 143.96814855965135) ##END= ##TITLE=Assignments ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR PEAK ASSIGNMENTS ##DATA CLASS=PEAK ASSIGNMENTS ##BLOCK_ID=4 ##CROSS REFERENCE=STRUCTURE:BLOCK_ID=1 ##TEMPERATURE=NA ##SOURCE REFERENCE=PMID 19212411 ##.OBSERVE FREQUENCY=600 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##NPOINTS=12 ##XUNITS=PPM ##PEAK ASSIGNMENTS=(XMA) (4.22,
, <16>) (4.22,
, <16>) (4.22,
, <16>) (4.22,
, <16>) (2.45,
, <17>) (2.45,
, <17>) (2.45,
, <17>) (2.45,
, <17>) (2.66,
, <18>) (2.66,
, <18>) (2.66,
, <18>) (2.66,
, <18>) ##END= ##END= ##TITLE=NP0000333, Submission ID 255, Experimental spectrum ##JCAMP-DX=4.24 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=LINK ##TITLE=Ureidosuccinic acid ##JCAMP-CS=3.7 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##BLOCK_ID=1 ##CROSS REFERENCE=NMR PEAK ASSIGNMENTS:BLOCK_ID=4 ##MOLFORM=C5 H8 N2 O5 ##ATOMLIST= 1 N 0 2 C 0 3 O 0 4 N 0 5 C 0 6 C 0 7 C 0 8 O 0 9 O 0 10 C 0 11 O 0 12 O 0 13 H 0 14 H 0 15 H 0 16 H 0 17 H 0 18 H 0 19 H 0 20 H 0 ##BONDLIST= 1 2 S 2 3 D 2 4 S 4 5 S 5 6 S 6 7 S 7 8 D 7 9 S 5 10 S 10 11 D 10 12 S 1 13 S 1 14 S 4 15 S 5 16 S 6 17 S 6 18 S 9 19 S 12 20 S ##STEREOCENTER= 5 P 0 ##$MOLFILE= RDKit 3D 20 19 0 0 0 0 0 0 0 0999 V2000 2.6936 1.6724 -0.3217 N 0 0 0 0 0 0 0 0 0 0 0 0 1.9742 0.5585 0.1827 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4492 -0.1306 1.0559 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6970 0.2702 -0.3653 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.1158 -0.8143 0.1732 C 0 0 1 0 0 0 0 0 0 0 0 0 -1.1277 -0.1826 1.1646 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9161 0.9028 0.6078 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.6870 1.5037 1.4410 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.9840 1.3707 -0.6800 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7377 -1.7169 -0.7547 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8715 -1.9297 -0.9644 O 0 0 0 0 0 0 0 0 0 0 0 0 0.1969 -2.4892 -1.5368 O 0 0 0 0 0 0 0 0 0 0 0 0 3.4029 1.6492 -1.0755 H 0 0 0 0 0 0 0 0 0 0 0 0 2.4948 2.5994 0.1934 H 0 0 0 0 0 0 0 0 0 0 0 0 0.3841 0.7655 -1.1966 H 0 0 0 0 0 0 0 0 0 0 0 0 0.5290 -1.4256 0.8654 H 0 0 0 0 0 0 0 0 0 0 0 0 -0.6367 0.0691 2.0715 H 0 0 0 0 0 0 0 0 0 0 0 0 -1.8475 -1.0499 1.3392 H 0 0 0 0 0 0 0 0 0 0 0 0 -2.8796 1.2387 -1.1326 H 0 0 0 0 0 0 0 0 0 0 0 0 0.9819 -2.8614 -1.0671 H 0 0 0 0 0 0 0 0 0 0 0 0 1 2 1 0 2 3 2 0 2 4 1 0 4 5 1 0 5 6 1 0 6 7 1 0 7 8 2 0 7 9 1 0 5 10 1 0 10 11 2 0 10 12 1 0 1 13 1 0 1 14 1 0 4 15 1 0 5 16 1 1 6 17 1 0 6 18 1 0 9 19 1 0 12 20 1 0 M END ##END= ##TITLE=Experimental spectrum ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR SPECTRUM ##BLOCK_ID=2 ##TEMPERATURE=NA ##.OBSERVE FREQUENCY=600 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##.SHIFT REFERENCE=INTERNAL,DSS,58937.00,0.0 ##XUNITS=PPM ##FIRSTX=10.803153756609914 ##LASTX=-1.2094135854575585 ##MINX=-1.2094135854575585 ##MAXX=10.803153756609914 ##XFACTOR=0.00018330002810884594 ##NPOINTS=65536 ##YUNITS=ARBITRARY UNITS ##FIRSTY=0.5219995558674096 ##LASTY=-5.004298476447707e-05 ##MINY=-830.992253485301 ##MAXY=10000.0 ##YFACTOR=0.3051850947599719 ##XYDATA=(X++(Y..Y)), XYDATA $$ DIF 58937B%%%%j%%%%%%%%%%%%%%%%%%%%%%j%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58863@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58789@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58715@%%%%%j%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58641@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%j%%%%%%%%%%%%%%%J%%% 58567A%%%%%%%%%%%%%%%%J%%%%%%j%%%%%%%%J%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58493A%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%% 58419A%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58345@%%%%%%%%%%j%%%%%%%J%%%%%%%%%%j%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 58271@%%%%%%%%%%%%%%%%%%%%%%%%%%j%J%%%%%%%j%%%%%%%%%J%%%%%%j%%%J%%%%%%%%%%%%%%%% 58197@%%%%%%%%%%%j%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%j%%%%% 58123@%%%%%%%%%%%%%%%%%%%%%%%%J%%%%j%%%%%J%%%j%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%j%% 58049@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%J%%%%%%%%% 57975@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%J%%%j%%J%%%%%%%%%% 57901@%%%%%%%%%%%%%%%%%j%%%%J%%%%%%%%%j%%%%%%%%%%%j%%%%%%J%%%%%%%J%%%%j%%J%%%%%% 57827@%j%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 57753@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J% 57679Aj%%%%%J%j%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%J% 57605a%%%j%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%% 57531@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%J%%%%j%%%%% 57457A%%%%%j%%%%%%%%%%j%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%J%%%%%% 57383@%%%%%%%%%%%%%%%%%%j%%%%%%%%%J%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%% 57309@%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%j%%%%%%%%%% 57235A%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%j%%%%%%%%J%%%j%%%%%%%%%%%%%%%%%%%J%%%%%%%%%% 57161@%j%%J%%%%%%%%jJ%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%% 57087@%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%j%%%%%%%%J%% 57013@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 56939@%%%%%%%%%%%%%%%J%%j%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 56865aJ%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%j%%%%%%%%%%%%%%%%j 56791a%%%%%%%%%%%%%%%%%J%%%%%%%j%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%J%%%%%j% 56717@%J%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%Jj%%%% 56643Aj%%%%J%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%j%%%%%%%%%%J% 56569a%%%j%%%%%%J%j%%%J%%%%%%%%j%%%%%%%%%J%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%j 56495c%J%%%%%%%%%%%%%%%%%%%%%%J%%%%%j%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%J%%%%%%%%%%% 56421@%%%%%%%%%%%%%%%j%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%J%%%%%%%%%% 56347@%%%%%%%%%%%%%%%%%%%j%%J%%%%%jJ%%%%%%%%%%J%%%%%%%%%%%%%%%%j%%J%%%%%%%%j%%%% 56273@%%%%%%%%%%%%%%J%%%%%%%%%%%%%%j%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%% 56199@%%%%%%%%j%%%%%%%%%%%%%%%%%j%%%J%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 56125@%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%J%%%%%%%%%%%J%%%%j%% 56051a%%%%%J%%%%%%%%%%%%%%%j%%%%%%%%%%%%%Jj%%%%J%%%%%j%%%%%%%J%%%j%%%%%%%%%J%%%% 55977@%%%%%%%%J%%%%%%%j%%%%%%%%%%%%%%%%%%%j%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%% 55903A%%%%j%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%j%%J%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%% 55829@%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%% 55755A%%%%%%%%%J%%%%%%%%j%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%j%J%%%%%%%%%%%%%%% 55681@%%%%%%%%%%%%%%%%%%%%%%%J%%%j%%%%%%j%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%% 55607@%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%j%%%J%% 55533A%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%jJ%%%%j%%%%%%%J%%%%%%%J%%%%%%%%%%j%%%%%%%J%% 55459A%%%%%%%%%%j%%%%J%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%j%%J%%%%%%%j%%%%%%%%%%%% 55385a%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%J%%%%%j%%%%%%J%%j%%%%%J%%%%%%%%%%%%%%%jJ% 55311A%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 55237A%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%j%%%%%%%%%%%%%%J%%%%%%% 55163A%%%%%jJ%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%j%%%%%%%%%%%%%%%j%%%%%%% 55089@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 55015@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%J%%%%%%%% 54941@%%%%%%j%%%%%%%%%J%%%%%%%%%%%%%%%%%J%%%%%jJ%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%% 54867@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%% 54793@%%%%%%%J%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%j 54719@%%%%%%%%J%%%%%%%%%%%%%%%%j%%%%%%%%Jj%%%%%J%%%%%%%%%%%%%%%%%%%j%%%%%J%%%%j% 54645@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%% 54571a%%%%%%%%%%%%%%%%%%%%%%%%Jj%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%% 54497a%%%J%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 54423a%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%j%%%j%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%% 54349@%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%J%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%% 54275a%%%%%%J%%%j%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%j%%%% 54201@%%%%%%j%%%%%%%J%%%%%%%%%%%%%%%j%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%% 54127Aj%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%J%%%%%%%%%%% 54053A%%%%%%J%%%%%%%%%%%j%%%%%%%%%J%%%%%%%%j%%%%%%%%%%%%%%%%%%%%j%%%%%%%%J%%%%%% 53979A%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%Jj%%%%%%%%%%%%%%%%%%%%%%% 53905B%%%%%j%%%%%%%%%J%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%% 53831@%%%%%%J%%%%%j%%%%%J%%%%%%%%%%%j%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%Jj%%%%%%J%%% 53757B%%%j%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%j%%%%%%%J%%%%%%%%%%%%%j%%%%%%%J% 53683@%%%%%%%j%%%J%j%%J%%%%%%%%%%%%%%%j%%%%%%%%%J%%j%%%%%%J%%%%%%%%%%%%%%%%%%%%% 53609@%%%%%%%%%%%%%%%%%%J%%%%%%%%%j%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%% 53535@%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%% 53461A%%%%%%%%j%%%%%%%%%%%%%%%%%%%%j%%%%%%J%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%J%%%% 53387@%%%%%%%%%%%%%%%%%%%%%jJ%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 53313@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%j%%%%%%% 53239b%%%%%%%J%%%%%%%%j%%J%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%j%%%%%%%%%%%J%%%%%%%j 53165c%%%%%J%%%%%j%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%J%%%%%% 53091@%%%j%%%%J%%%%%%%%%%%%%%%%%%%%j%%%%%J%%%%%%%j%%%%%%%%%%%%%%%%%%%j%%%%%%%%%% 53017b%%%%Jj%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%J%%%%%%%% 52943a%%j%%%%%%%%%%J%%j%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%J%%%%%% 52869aj%%%%J%%%%%%J%%%%%j%%%%%%%%J%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%% 52795b%%%%J%%%%%%J%%%%%%%%%J%%%%%%%%%%j%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%jJ%%%%%%%% 52721A%%%%j%%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%% 52647A%%%%%j%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%% 52573@%j%%J%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%J%%%%%%%%%%%%%%%J%%%%%j%%%%%%%%%%%%%%%% 52499@%%%%%%%%%%%%%J%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%J%%%%%%%%%%%%%%%%%%%%%% 52425@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 52351@%%%%%%%%%%%%%j%%%%%%%%%%%J%%%%%%%%%%%j%%%%%%J%%%%%%%%j%%%%%%%%%%%%%%%%%%%% 52277a%%%%J%%%%%%%%j%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%J%%%%%%%%%j%%%%%%J%%%%%%% 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44211@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%% 44137a%J%%%%%%%%%%%%%%%%%%%%J%%%%%%%J%%%%%%%%%%J%%%%%%%%%%%%j%%%%j%%%%%%%%%%%%%% 44063A%%%%%%%%%%%%%%%%%%%%%%%%%%%J%j%%%%j%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%% 43989@j%%%%%%%J%%%%%%%j%%%%%%%%%%%%%%%J%%J%%%%%%%%%%%%%%%j%%%%J%%%%%%%%%%%%%%%%% 43915A%J%%%%%%%%%j%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%j%%%%%%%%%%%%%%j%%% 43841AJ%%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%j%%%%%% 43767@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 43693@%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%j%J%%%%%%%%%%%%%j%%%%J%%%%%%%%%%%%%%%j% 43619@%%%%J%%%%%%%%%%%%%J%%%%%%%%%%%%%%%%%J%%%%%%%%j%%%%%%%%%%%%%%%%%%%%Jj%%%%%% 43545B%%%%%%%%%%%J%%%%%j%%%%%%J%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%j%%%%%%%%%%%j%%%% 43471@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 43397@%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%J%%%%%%%%%%%j%%%J%%%%j%%%%%%%%%%%%%%%%%%%j% 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-5451A%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%J%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5525@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5599@%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%j%%%%%J%%%%%%%%%%%%%% -5673a%%%%%J%%%%%%%%%%%%%%%%%J%%%%%%%%j%%%%%%%%%%%%%%%%%%%%J%%%j%%%%%%%%%%%%%%%% -5747@%%%%%%%%%%%%%J%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%J%%%%%%%%%%%%%%%%%%%%%% -5821@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -5895@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%%%%%%%J -5969@%%%%%j%%%%%%%%%%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6043@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%J%%%%%%%%%%%%%% -6117@%%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%J%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6191A%%%%%%%%%%%%%%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6265@%%%%%%%%%%%%%%J%%%%%%%%%J%j%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%j%%%%%%%%% -6339@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6413@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6487@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6561@%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6598@ $$ checkpoint ##END= ##TITLE=Simulated peaks ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR PEAK TABLE ##DATA CLASS=PEAK TABLE ##BLOCK_ID=3 ##TEMPERATURE=NA ##.OBSERVE FREQUENCY=600 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##NPOINTS=12 ##XUNITS=PPM ##YUNITS=ARBITRARY UNITS ##PEAK TABLE=(XY..XY) (4.2335205078125, 144.13035990246647) (4.2257232666015625, 144.85347701644844) (4.2141876220703125, 145.14651189489348) (4.2064971923828125, 144.34524705475368) (2.475082397460937, 142.00913805870258) (2.455856323242187, 142.65802460882202) (2.4442138671874996, 143.05740586188728) (2.4249877929687496, 141.8331438753004) (2.679306030273437, 144.0049516400396) (2.671615600585937, 144.12603948222895) (2.6484374999999996, 144.1830356293766) (2.6407470703124996, 143.96814855965135) ##END= ##TITLE=Assignments ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR PEAK ASSIGNMENTS ##DATA CLASS=PEAK ASSIGNMENTS ##BLOCK_ID=4 ##CROSS REFERENCE=STRUCTURE:BLOCK_ID=1 ##TEMPERATURE=NA ##SOURCE REFERENCE=PMID 19212411 ##.OBSERVE FREQUENCY=600 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##NPOINTS=12 ##XUNITS=PPM ##PEAK ASSIGNMENTS=(XMA) (4.22,
, <16>) (4.22,
, <16>) (4.22,
, <16>) (4.22,
, <16>) (2.45,
, <17>) (2.45,
, <17>) (2.45,
, <17>) (2.45,
, <17>) (2.66,
, <18>) (2.66,
, <18>) (2.66,
, <18>) (2.66,
, <18>) ##END= ##END=